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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 643926Generated: October 31, 2026

Trifluoroacetic acid → HCID 66750776, compound

https://huagongshe.com/reaction/643926

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 66750652HCID 66750652—
SolventDichloromethaneHCID 6344—
ProductHCID 66750776HCID 66750776—

Reaction Steps

To a solution of 5-(6-benzyloxy-2-methyl-2,3-dihydrobenzo[b]thiophen-5-yl)-2-(2,4-dimethoxybenzyl)-1,1-dioxo-1,2,5-thiadiazolidin-3-one (71 mg, 0.13 mmol) in DCM (8 mL) is added TFA (10 mL) and the mixture is stirred at RT for 4 h. TFA and DCM are removed under vacuum to give the title compound and it is used directly in the next step: (M+H)+=301.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07700633B2
Source datasetuspto-grants-2010_04
ORD IDord-fbf23991cbc0476d95c8e9064e06eaf9
Source noteuspto-grants-2010_04