HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 66750538, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 66750840 | HCID 66750840 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 66750538 | HCID 66750538 | — |
Reaction Steps
To a solution of 5-benzyloxy-6-(1,1,4-trioxo-1,2,5-thiadiazolidin-2-yl)-1H-indole-2-carboxylic acid ethyl ester (from Example 65) (0.135 g, 0.398 mmol) in water (8 mL) is added 1M KOH (0.29 mL). The solution is stirred at room temperature for 1 h. The reaction product is lyophilized to yield 5-benzyloxy-6-(1,1,4-trioxo-1,2,5-thiadiazolidin-2-yl)-1H-indole-2-carboxylic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07700633B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-0e0fc1b747d449e8ae85d5033d037a41 |
| Source note | uspto-grants-2010_04 |