HuagongsheHuagongshe Chemistry Print Report · For research reference only
AURORA 623 → HCID 43576350, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | AURORA 623 | HCID 721284 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 43576350 | HCID 43576350 | — |
Reaction Steps
A solution of the title A compound, 2-(4-nitro-benzenesulfonylamino)-benzoic acid methyl ester (1 g, 2.98 mmol) in 40 mL of ethanol containing 0.32 g of 10% palladium on carbon is shaken under 40 psi of hydrogen pressure at RT for 2.5 h. The mixture is filtered and concentrated under vacuum to give 2-(4-amino-benzenesulfonyl-amino)-benzoic acid methyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07700637B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-e7b4f166e48b48f797023784d272dfc6 |
| Source note | uspto-grants-2010_04 |