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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 644198Generated: October 30, 2026

Potassium Carbonate → HCID 57860852, compound

https://huagongshe.com/reaction/644198

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 68530931HCID 68530931—
SolventMorpholineHCID 8083—
ProductHCID 57860852HCID 57860852—

Reaction Conditions

Temperature100 °C

Reaction Steps

A mixture of 2-[2-(2-tert-butoxycarbonylaminoethoxy)-4-fluorobenzoylamino]-N-(5-chloropyridin-2-yl)-5-fluorobenzamide (0.8 g, 1.5 mmol), morpholine (10 mL), and K2CO3 (0.2 g) was heated in a sealed tube at 100° C. for 12 hours and then 120° C. for 4 h.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07700628B2
Source datasetuspto-grants-2010_04
ORD IDord-21920d70d5eb46f6b6722c99e6fdb589
Source noteuspto-grants-2010_04