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HRID644221

反应详情

EQUATION

反应方程式

HRID 644221 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)c1ccc(F)cc1O
HCID2775386

methyl 4-fluoro-2-hydroxybenzoate

C8H7FO3

结构：CC(C)(C)OC(=O)NCCCO
HCID3838134

3-(Boc-amino)-1-propanol

C8H17NO3

PRODUCTS

生成物

1
结构：COC(=O)c1ccc(F)cc1OCCCNC(=O)OC(C)(C)C
HCID57602453

未命名化合物

收率 84%

PROCEDURE

实验过程

Using a procedure analogous to Example 1-C, methyl 2-hydroxy-4-fluorobenzoate and 3-(tert-butoxycarbonylamino)propanol gave the desired product as a white solid (20.6 g, 84%). 1NMR IS-MS, m/e: 328 (m+1).