2-Amino-5-chloro-N-(5-chloropyridin-2-yl)benzamide → 2-[2-[2-(tert-Butoxycarbonylamino)ethoxy]-4-(methylthio)benzoylamino]-5-chloro-N-(5-chloropyridin-2-yl)benzamide

Participants

Role	Name	HCID	Charge
Reactant	2-Amino-5-chloro-N-(5-chloropyridin-2-yl)benzamide	HCID 21906418	—
Reactant	2-(2-Tert-butoxycarbonylaminoethoxy)-4-(methylthio)benzoic acid	HCID 57936572	—
Product	2-[2-[2-(tert-Butoxycarbonylamino)ethoxy]-4-(methylthio)benzoylamino]-5-chloro-N-(5-chloropyridin-2-yl)benzamide	HCID 68533941	—

Reaction Steps

2-[2-[2-(tert-Butoxycarbonylamino)ethoxy]-4-(methylthio)benzoylamino]-5-chloro-N-(5-chloropyridin-2-yl)benzamide was prepared by methods described in example 4-E from 2-[2-(tert-butoxycarbonylamino)ethoxy]-4-(methylthio)benzoic acid and N-(5-chloropyridin-2-yl)-2-amino-5-chlorobenzamide (3 g, 92%). IR (CHCl3): 1665, 1500, 1375, 1296 cm−1.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07700628B2
Source dataset	uspto-grants-2010_04
ORD ID	ord-0a71aaa0a1404b9ba18a2aafd1b9ce7b
Source note	uspto-grants-2010_04