反应详情

A mixture of 29.2 g (87.6 mmol) monoethyl 2-acetylamino-2-(5,6,7,8-tetrahydro-naphthalen-2-ylmethyl)-malonate and 400 mL toluene was refluxed for 5 h. The reaction mixture was then washed with 1 M NaOH and water, dried and evaporated down under reduced pressure.

1. temperaturewas refluxed for 5 h
2. washThe reaction mixture was then washed with 1 M NaOH and water
3. customdried
4. customevaporated down under reduced pressure