HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1,1-Trifluoro-5,5-dimethyl-2,4-hexanedione → 5-(tert-Butyl)-1-(4-nitrophenyl)-3-(trifluoromethyl)pyrazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1,1-Trifluoro-5,5-dimethyl-2,4-hexanedione | HCID 89830 | — |
| Reactant | 4-Nitrophenylhydrazine hydrochloride | HCID 5463401 | — |
| Product | 5-(tert-Butyl)-1-(4-nitrophenyl)-3-(trifluoromethyl)pyrazole | HCID 18677147 | 94.7% |
Reaction Steps
Using 1,1,1-trifluoro-5,5-dimethyl-2,4-hexanedione and 4-nitrophenylhydrazine hydrochloride as the raw materials, the same operation as the Example 538(1) gave the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07700655B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-eba3089427ee4a3697ff0375ed43d87f |
| Source note | uspto-grants-2010_04 |