Dimethylamine → HCID 11165474, compound

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This was prepared analogously to 5-Ethoxycarbonyl-7-(3-(morpholin-4-yl-methyl)phenyl)-1-phenylbenzimidazole from 5-ethoxycarbonyl-7-(3-(chloromethyl)phenyl)-1-phenylbenzimidazole (0.50 g, 1.28 mmol) and dimethylamine (approximately 2 ml) in anhydrous dimethylformamide (5 ml). The crude product was triturated in diethyl ether to afford the title product as an off-white solid (0.139, 25%) m/z, 400.2 (M+H)+.

Provenance & Evidence