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HRID64472

反应详情

EQUATION

反应方程式

HRID 64472 的结构方程式

REACTANTS

反应物

2
结构：CCOC(C)=O.Cl
HCID21866389

未命名化合物

结构：Cc1nc2c(OCC3CCCCC3)cccn2c1C(=O)N[C@H]1CCN(C)C1
HCID71478936

未命名化合物

PRODUCTS

生成物

1
结构：Cc1nc2c(OCC3CCCCC3)cccn2c1C(=O)N[C@H]1CCN(C)C1.Cl
HCID86713499

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

To 245 mg of 8-(cyclohexylmethoxy)-2-methyl-N-[(3S)-1-methylpyrrolidin-3-yl]imidazo[1,2-a]pyridine-3-carboxamide were added 12 ml of ethyl acetate and 364 μl of a 4 M hydrogen chloride/ethyl acetate solution, followed by stirring. The resulting solid was collected by filtration and dried to obtain 258 mg of 8-(cyclohexylmethoxy)-2-methyl-N-[(3S)-1-methylpyrrolidin-3-yl]imidazo[1,2-a]pyridine-3-carboxamide hydrochloride.

WORKUP

后处理

  1. filtrationThe resulting solid was collected by filtration
  2. customdried