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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 644743Generated: October 30, 2026

tert-Butyl methylcarbamate → 1,1-Dimethylethyl (4-formyl-3-methylphenyl)methylcarbamate

https://huagongshe.com/reaction/644743

Reaction equation

Participants

RoleNameHCIDCharge
Reactanttert-Butyl methylcarbamateHCID 527635—
Reactant4-Bromo-2-methylbenzaldehydeHCID 13555150—
Product1,1-Dimethylethyl (4-formyl-3-methylphenyl)methylcarbamateHCID 86618112—

Reaction Steps

The title compound was prepared from crude 4-bromo-2-methylbenzaldehyde (D91) and 1,1-dimethylethyl methylcarbamate (D83) using a method similar to that described for D84 in Description 84. δH (CDCl3, 400 MHz) 10.20 (1H, s), 7.76 (1H, d), 7.28 (1H, dd), 7.19 (1H, d), 3.31 (3H, s), 2.66 (3H, s), 1.49 (9H, s).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07700599B2
Source datasetuspto-grants-2010_04
ORD IDord-a40fb7f683f64bb291d5ebb794f090bb
Source noteuspto-grants-2010_04