HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium formate → HCID 58662440, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium formate | HCID 2723923 | — |
| Reactant | HCID 58662444 | HCID 58662444 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 58662440 | HCID 58662440 | — |
Reaction Steps
This compound can be obtained by reacting a solution of 2-ethyl-6,8-dimethyl-4-oxo-3,4-dihydro-2H-[1,7]naphthyridine-1-carboxylic acid benzyl ester in methanol, under nitrogen atmosphere, with ammonium formate (2.5 eqv) and 10% Pd—C (50% water wet), at about 40° C. for a time period of about 1 h, followed by a typical workup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07700774B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-d523029be6f449e88091244dabee8b7f |
| Source note | uspto-grants-2010_04 |