HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → HCID 58662430, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 58662440 | HCID 58662440 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 58662430 | HCID 58662430 | — |
Reaction Steps
This compound can be obtained by reacting a suspension of K2CO3 (3-5 eqv) in THF with a solution of 2-ethyl-6,8-dimethyl-2,3-dihydro-1H-[1,7]naphthyridin-4-one in THF and ethyl chloroformate (1.5 to 2 eqv), typically at a temperature from about RT to about 50° C., followed by a typical workup procedure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07700774B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-163bd8070ba94b1084db943b308ef5b8 |
| Source note | uspto-grants-2010_04 |