HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 136385125, compound → HCID 58662425, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 136385125 | HCID 136385125 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 58662425 | HCID 58662425 | — |
Reaction Steps
This compound can be prepared by reacting a solution of 2-ethyl-4-hydroxyimino-6,8-dimethyl-3,4-dihydro-2H-[1,7]naphthyridine-1-carboxylic acid ethyl ester in acetic acid with Zn (5 to 10 eqv), typically at reflux temperature, for about 1 h to about 5 h, followed by a typical workup procedure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07700774B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-64b9e4aebf85417d820911c308b9e13a |
| Source note | uspto-grants-2010_04 |