HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl chloroformate → HCID 11526955, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl chloroformate | HCID 6586 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 58662428 | HCID 58662428 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 11526955 | HCID 11526955 | — |
Reaction Steps
This compound can be prepared by reacting, a solution of 4-(3,5-bis-trifluoromethyl-benzylamino)-2-ethyl-6,8-dimethyl-3,4-dihydro-2H-[1,7]naphthyridine-1-carboxylic acid ethyl ester in THF and K2CO3 (2 to 5 eqv) with methyl chloroformate, followed by a typical workup procedure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07700774B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-3d15413279a94b3782aa8b244e0e2a9a |
| Source note | uspto-grants-2010_04 |