HRID645114

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID68289

Sesamol

C7H6O3

结构：O=C1C(=O)N(C(c2ccccc2)c2ccccc2)c2ccccc21

HCID1969277

1-(diphenylmethyl)-1H-indole-2,3-dione

C21H15NO2

HCID2733261

3-(Trifluoromethoxy)phenol

C7H5F3O2

HCID65596570

未命名化合物

PRODUCTS

生成物

结构：O=C1N(C(c2ccccc2)c2ccccc2)c2ccccc2C1(O)c1ccc(OC(F)(F)F)cc1O

HCID12004334

未命名化合物

PROCEDURE

实验过程

Following the procedure as described in PREPARATION 2B, and making non-critical variations to replace 1-(2-cyclopropylethyl)-1H-indole-2,3-dione with 1-(diphenylmethyl)-1H-indole-2,3-dione, and 1,3-benzodioxol-5-ol with 3-(trifluoromethoxy)phenol, the title compound was obtained (75%): MS (ES+) m/z 514.5 (M+23).

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-db27bfbf6b374dbcbd78a6113dcd43e8
来源数据集: uspto-grants-2010_04
DOI: 10.6084/m9.figshare.5104873.v1
专利: US07700641B2
来源说明: uspto-grants-2010_04

反应 SMILES

C1(CCN2C3C(=CC=CC=3)C(=O)C2=O)CC1.[C:17]1([CH:23]([C:35]2[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=2)[N:24]2[C:32]3[C:27](=[CH:28][CH:29]=[CH:30][CH:31]=3)[C:26](=[O:33])[C:25]2=[O:34])[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1.O1C2C=CC(O)=CC=2OC1.[F:51][C:52]([F:62])([F:61])[O:53][C:54]1[CH:55]=[C:56]([OH:60])[CH:57]=[CH:58][CH:59]=1>>[C:35]1([CH:23]([C:17]2[CH:18]=[CH:19][CH:20]=[CH:21][CH:22]=2)[N:24]2[C:32]3[C:27](=[CH:28][CH:29]=[CH:30][CH:31]=3)[C:26]([OH:33])([C:57]3[CH:58]=[CH:59][C:54]([O:53][C:52]([F:61])([F:62])[F:51])=[CH:55][C:56]=3[OH:60])[C:25]2=[O:34])[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=1