Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sesamol → 1-(diphenylmethyl)-3-hydroxy-3-[2-hydroxy-4-(trifluoromethoxy)phenyl]-1,3-dihydro-2H-indol-2-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sesamol | HCID 68289 | — |
| 반응물 | 1-(diphenylmethyl)-1H-indole-2,3-dione | HCID 1969277 | — |
| 반응물 | 3-(Trifluoromethoxy)phenol | HCID 2733261 | — |
| 반응물 | 1-(2-cyclopropylethyl)-1H-indole-2,3-dione | HCID 65596570 | — |
| 생성물 | 1-(diphenylmethyl)-3-hydroxy-3-[2-hydroxy-4-(trifluoromethoxy)phenyl]-1,3-dihydro-2H-indol-2-one | HCID 12004334 | — |
반응 단계
Following the procedure as described in PREPARATION 2B, and making non-critical variations to replace 1-(2-cyclopropylethyl)-1H-indole-2,3-dione with 1-(diphenylmethyl)-1H-indole-2,3-dione, and 1,3-benzodioxol-5-ol with 3-(trifluoromethoxy)phenol, the title compound was obtained (75%): MS (ES+) m/z 514.5 (M+23).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07700641B2 |
| 출처 데이터셋 | uspto-grants-2010_04 |
| ORD ID | ord-db27bfbf6b374dbcbd78a6113dcd43e8 |
| 출처 메모 | uspto-grants-2010_04 |