HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 645485Generated: October 30, 2026
HCID 68708639, compound → tert-Butyl [(4-phenylpiperidin-4-yl)methyl]carbamate
https://huagongshe.com/reaction/645485
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 68708639 | HCID 68708639 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | tert-Butyl [(4-phenylpiperidin-4-yl)methyl]carbamate | HCID 49760176 | — |
Reaction Steps
A mixture of 4-(tert-butoxycarbonylaminomethyl)-4-phenylpiperidine-1-carboxylic acid 1-chloroethyl ester in MeOH is stirred at 60° C. for 5 h, then the reaction mixture is concentrated in vacuo to give (4-phenylpiperidin-4-ylmethyl) carbamic acid tert-butyl ester, which is directly used for the next reaction without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07704996B2 |
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| Source dataset | uspto-grants-2010_04 |
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| ORD ID | ord-e4ad7842bfac4539befd6deb0806c9ab |
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| Source note | uspto-grants-2010_04 |
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