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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 645487Generated: October 29, 2026

Hydrochloric Acid → HCID 68706690, compound

https://huagongshe.com/reaction/645487

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 68706126HCID 68706126—
SolventDiethyl EtherHCID 3283—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 68706690HCID 68706690—

Reaction Steps

To a solution of (1-acetyl-4-phenylpiperidin-4-ylmethyl)carbamic acid tert-butyl ester in ether is added 4 N HCl in 1,4-dioxane. The reaction mixture is stirred at room temperature for 1 h, and concentrated in vacuo. The resulting solid is washed with ether to give the title compound, which is directly used for the next reaction without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07704996B2
Source datasetuspto-grants-2010_04
ORD IDord-eb968db4ea084ac79dd1ef5970d10c29
Source noteuspto-grants-2010_04