HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68706690, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 68706126 | HCID 68706126 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 68706690 | HCID 68706690 | — |
Reaction Steps
To a solution of (1-acetyl-4-phenylpiperidin-4-ylmethyl)carbamic acid tert-butyl ester in ether is added 4 N HCl in 1,4-dioxane. The reaction mixture is stirred at room temperature for 1 h, and concentrated in vacuo. The resulting solid is washed with ether to give the title compound, which is directly used for the next reaction without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07704996B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-eb968db4ea084ac79dd1ef5970d10c29 |
| Source note | uspto-grants-2010_04 |