HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloronicotinonitrile → HCID 68583656, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloronicotinonitrile | HCID 81079 | — |
| Reactant | 4-(Trifluoromethoxy)phenylboronic acid | HCID 2734386 | — |
| Product | HCID 68583656 | HCID 68583656 | 70% |
Reaction Steps
Prepared in 70% yield from 2-chloro-3-cyanopyridine and 4-trifluoromethoxyphenylboronic acid according to the procedure described for Example 153A. MS (ESI−) m/z 265.0 (M+H)+; 1H NMR (CDCl3) δ 7.37-7.44 (m, 3H), 7.98-8.03 (m, 2H), 8.10 (dd, J=8.0, 1.9 Hz, 1H), 8.89 (dd, J=4.7, 1.7 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07704997B1 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-98108807571f43d2aeaf69e9d32824c6 |
| Source note | uspto-grants-2010_04 |