HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Chlorophenyl)pyrrolidine → HCID 68582409, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Chlorophenyl)pyrrolidine | HCID 592391 | — |
| Reactant | HCID 59689467 | HCID 59689467 | — |
| Product | HCID 68582409 | HCID 68582409 | 10.1% |
Reaction Steps
The compound from Example 75B (0.1 g) was reacted with 2-(4-Chloro-phenyl)-pyrrolidine (0.1 g) according to the method of Example 75C to provide 0.016 g of the title compound as a white solid. MS (ESI/NH3) m/z 395 (M+H)+; 1H NMR (δ, DMSO-d6) 1.78-1.9 (m, 4H), 3.3-3.6 (m, 2H), 4.8-5.0 (m, 1H) 6.8-6.9 (m, 1H), 7.05-7.19 (m, 4H), 7.60-7.65 (t, 1H), 7.79-7.85 (d, 1H), 7.99-8.1 (d, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07704997B1 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-fa80057b5f09408a8bee65fbaed0524b |
| Source note | uspto-grants-2010_04 |