HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 5-aminocarbonyl-4,6-dimethoxy-2-(trifluoromethyl)-3-pyridinecarboxylate → HCID 13726807, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 5-aminocarbonyl-4,6-dimethoxy-2-(trifluoromethyl)-3-pyridinecarboxylate | HCID 13726804 | — |
| Solvent | Phosphorus oxychloride | HCID 24813 | — |
| Product | HCID 13726807 | HCID 13726807 | 84.9% |
Reaction Steps
This material was obtained in 84.9% yield from the product of Example 22 (0.014 mol) and 100 ml of POCl3 by a procedure similar to that in Example 24 as a solid: mp 32°-34° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04609399 |
| Source dataset | uspto-grants-1986_09 |
| ORD ID | ord-e12071271bcf433eb2bc478899e6d6fb |
| Source note | uspto-grants-1986_09 |