HRID64572

反应详情

EQUATION

反应方程式

HRID 64572 的结构方程式

REACTANTS

反应物

1

结构：CCOC(=O)c1c(C(F)(F)F)nc(OC)c(C(N)=O)c1OC

未命名化合物

PRODUCTS

生成物

1

结构：CCOC(=O)c1c(C(F)(F)F)nc(OC)c(C#N)c1OC

未命名化合物

收率 84.9%

AUXILIARIES

试剂、催化剂与溶剂

1

结构：O=P(Cl)(Cl)Cl

溶剂HCID24813

Phosphoric trichloride

Cl3OP

PROCEDURE

实验过程

This material was obtained in 84.9% yield from the product of Example 22 (0.014 mol) and 100 ml of POCl3 by a procedure similar to that in Example 24 as a solid: mp 32°-34° C.