HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3,5-Dimethyl-benzo[b]thiophen-2-yl)-phenyl-methanol → 2-[(3,5-Dimethyl-benzo[b]thiophen-2-yl)-phenyl-methyl]-3-hydroxy-4-methyl-4-phenyl-cyclobut-2-enone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3,5-Dimethyl-benzo[b]thiophen-2-yl)-phenyl-methanol | HCID 68579524 | — |
| Reactant | 2-Methyl-2-phenyl-cyclobutane-1,3-dione | HCID 68581027 | — |
| Product | 2-[(3,5-Dimethyl-benzo[b]thiophen-2-yl)-phenyl-methyl]-3-hydroxy-4-methyl-4-phenyl-cyclobut-2-enone | HCID 59264910 | — |
Reaction Steps
23.2 Using general procedure D, 2-methyl-2-phenyl-cyclobutane-1,3-dione (Lit. 1) was reacted with (3,5-dimethyl-benzo[b]thiophen-2-yl)-phenyl-methanol to give the title compound as a colorless solid. MS: 423.5 ([M−H]−).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07705034B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-82de5354ed89456b976383ca71cb3022 |
| Source note | uspto-grants-2010_04 |