HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 45923264, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-(4-Bromophenoxy)-2-methylpropanoic acid | HCID 344894 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 45923264 | HCID 45923264 | 78% |
Reaction Steps
A mixture of 2-(4-bromophenoxy)-2-methylpropanoic acid (10.0 g, 38.6 mmol). DMF (0.5 mL) and SOCl2 (40 mL) was heated for 3 h, allowed to cool and distilled to yield the sub-title compound (8.4 g, 78%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07705023B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-d78c7287691f4c90ba67b6ddc78af454 |
| Source note | uspto-grants-2010_04 |