HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 21186339, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | 2-(4-Bromophenoxy)-2-methylpropanoic acid | HCID 344894 | — |
| Product | HCID 21186339 | HCID 21186339 | 85% |
Reaction Steps
The sub-title compound was prepared by reduction of 2-(4-bromophenoxy)-2-methylpropanoic acid (2 g, 7.7 mmol) with BH3×THF (1M, 27.0 mmol, 27.0 mL) in accordance with the procedure described in Example 29(b). Distillation under reduced pressure gave the sub-title compound (1.60 g, 85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07705023B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-ed1c25f473c1460c94f17a383a716c67 |
| Source note | uspto-grants-2010_04 |