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HRID646446

反应详情

EQUATION

反应方程式

HRID 646446 的结构方程式

REACTANTS

反应物

2
结构：Cn1ccnc1Br
HCID2773262

2-Bromo-1-methyl-1H-imidazole

C4H5BrN2

结构：C[C@@H]1CCCN1C[C@@H]1CCCN1C(=O)c1ccc(B2OC(C)(C)C(C)(C)O2)cc1
HCID57980025

未命名化合物

PRODUCTS

生成物

1
结构：C[C@@H]1CCCN1C[C@@H]1CCCN1C(=O)c1ccc(-c2nccn2C)cc1
HCID59264668

未命名化合物

收率 11%

PROCEDURE

实验过程

The title compound is prepared in a manner substantially analogous to General Procedure A using [2-(S)-(2-(R)-methyl-pyrrolidin-1-ylmethyl)-pyrrolidin-1-yl]-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-methanone (439 mg, 1.1 mmol) and 2-Bromo-1-methyl-1H-imidazole (CAS 16681-59-7) (161 mg, 1.0 mmol) to give 39 mg (11% yield). MS (ES+) 353.2 (M+H)+

WORKUP

后处理

  1. customto give 39 mg (11% yield)