HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → N-benzyl-5-bromonicotinamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | 5-Bromonicotinic acid | HCID 88707 | — |
| Product | N-benzyl-5-bromonicotinamide | HCID 835760 | 90% |
Reaction Steps
5-bromo-N-(phenylmethyl)pyridine-3-carboxamide was synthesized according to the procedure described above from 5-bromonicotinic acid and benzylamine. Yield 90%. 1H NMR (400 MHz, CDCl3): 8.83 (d, 1H), 8.72 (d, 1H), 8.25 (t, 1H), 7.30 (m, 5H), 6.58 (br s, 1H), 4.62 (d, 2H); MS (EI) for C13H11N2OBr: 291 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07704995B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-e8d645be75714ff194efb8a3b7068456 |
| Source note | uspto-grants-2010_04 |