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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 646707Generated: October 30, 2026

m-Bromobenzenesulphonyl chloride → HCID 41647239, compound

https://huagongshe.com/reaction/646707

Reaction equation

Participants

RoleNameHCIDCharge
Reactantm-Bromobenzenesulphonyl chlorideHCID 17943—
Reactant1-Aminoindane, (S)-HCID 7000084—
ProductHCID 41647239HCID 4164723952%

Reaction Steps

3-bromo-N-[(1S)-2,3-dihydro-1H-indene-1-yl]benzenesulfonamide was synthesized according to the procedure described above from (S)-1-aminoindan and 3-bromobenzensulfonyl chloride. Yield 52%. 1H NMR (400 MHz, CDCl3): 7.20 (m, 1H), 7.90 (dd, 1H), 7.80 (dd, 1H), 7.50 (t, 1H), 7.20 (m, 2H), 7.15 (m, 1H), 7.02 br d, 1H), 4.80 (t, 1H), 2.90(m, 1H), 2.70 (m, 1H), 2.20 (m, 1H), 1.70 (m, 1H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07704995B2
Source datasetuspto-grants-2010_04
ORD IDord-6526912a231e4273a9c8b881c2c4d2f5
Source noteuspto-grants-2010_04