HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Bromobenzenesulphonyl chloride → HCID 41647239, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Bromobenzenesulphonyl chloride | HCID 17943 | — |
| Reactant | 1-Aminoindane, (S)- | HCID 7000084 | — |
| Product | HCID 41647239 | HCID 41647239 | 52% |
Reaction Steps
3-bromo-N-[(1S)-2,3-dihydro-1H-indene-1-yl]benzenesulfonamide was synthesized according to the procedure described above from (S)-1-aminoindan and 3-bromobenzensulfonyl chloride. Yield 52%. 1H NMR (400 MHz, CDCl3): 7.20 (m, 1H), 7.90 (dd, 1H), 7.80 (dd, 1H), 7.50 (t, 1H), 7.20 (m, 2H), 7.15 (m, 1H), 7.02 br d, 1H), 4.80 (t, 1H), 2.90(m, 1H), 2.70 (m, 1H), 2.20 (m, 1H), 1.70 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07704995B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-6526912a231e4273a9c8b881c2c4d2f5 |
| Source note | uspto-grants-2010_04 |