HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Phenylenediamine → HCID 68650316, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Phenylenediamine | HCID 7243 | — |
| Reactant | HCID 58710602 | HCID 58710602 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 68650316 | HCID 68650316 | — |
Reaction Steps
A solution of 3-amino-6-(3-formylphenyl)-N-methylpyrazine-2-carboxamide (25.4 mg, 0.1 mmol) and 1,2-phenylendiamine in NMP (3 mL) was heated at 80° C. for 8 h. The solvent was removed and the residue was triturated with 0.1 M aquous hydrochloric acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07704995B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-965ad633130f4f1abb397cba5c65c3a5 |
| Source note | uspto-grants-2010_04 |