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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 646892Generated: October 30, 2026

HCID 68680769, compound → HCID 68683203, compound

https://huagongshe.com/reaction/646892

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68680769HCID 68680769—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 68683203HCID 68683203101.2%

Reaction Steps

Using a procedure similar to Example 23, step (a), 4-[3-(2,5-dimethyl-pyrrol-1-yl)-4-nitro-phenyl]-piperazine-1-carboxylic acid tert-butyl ester (35 mg, 0.08 mmol) was stirred in MeOH in the presence of 5% Pd—C (20 mg) to afford 30 mg (100%) of the title compound as an oil. Mass spectrum (ESI, m/z): Calcd. for C21H30N4O2, 371.2 (M+H), found 371.1.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07705042B2
Source datasetuspto-grants-2010_04
ORD IDord-0d041ecb0e744490b3dc6d59bde83546
Source noteuspto-grants-2010_04