HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68680769, compound → HCID 68683203, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68680769 | HCID 68680769 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68683203 | HCID 68683203 | 101.2% |
Reaction Steps
Using a procedure similar to Example 23, step (a), 4-[3-(2,5-dimethyl-pyrrol-1-yl)-4-nitro-phenyl]-piperazine-1-carboxylic acid tert-butyl ester (35 mg, 0.08 mmol) was stirred in MeOH in the presence of 5% Pd—C (20 mg) to afford 30 mg (100%) of the title compound as an oil. Mass spectrum (ESI, m/z): Calcd. for C21H30N4O2, 371.2 (M+H), found 371.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07705042B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-0d041ecb0e744490b3dc6d59bde83546 |
| Source note | uspto-grants-2010_04 |