HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → 4-Hydrazino 7-trifluoromethyl-quinoline hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 4-Chloro-7-(trifluoromethyl)quinoline | HCID 67668 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-Hydrazino 7-trifluoromethyl-quinoline hydrochloride | HCID 20485594 | — |
Reaction Steps
A mixture of 4-chloro-7-trifluoromethylquinoline (21.95 g.) in ethanol (100 ml.) and hydrazine hydrate (60 g.) was refluxed overnight. The solvent and the excess of reagent were removed in vacuo to give 4-hydrazino-7-trifluoromethylquinoline hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04407803 |
| Source dataset | uspto-grants-1983_10 |
| ORD ID | ord-6f700dd3996a4c5086e6c4a914ac98e0 |
| Source note | uspto-grants-1983_10 |