HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(4-phenyl-thiazol-2-yl)-oxamic acid → 2-Ethylthioethyl N-(4-phenyl-thiazol-2-yl)-oxamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(4-phenyl-thiazol-2-yl)-oxamic acid | HCID 4713520 | — |
| Reactant | Ethylthioethanol | HCID 19024902 | — |
| Product | 2-Ethylthioethyl N-(4-phenyl-thiazol-2-yl)-oxamate | HCID 20485675 | — |
Reaction Steps
Using a method similar to Example 12, 6.2 g of N-(4-phenyl-thiazol-2-yl)-oxamic acid and 6.6 g of ethylthioethanol give, after crystallization of the product from ethanol, 3.4 g of the compound of the formula I, with R1 =C6H5 and R2 =CH2CH2SC2H5, of melting point 148°-149° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04407810 |
| Source dataset | uspto-grants-1983_10 |
| ORD ID | ord-c24a988f795142e7a3c200ce844561a8 |
| Source note | uspto-grants-1983_10 |