Methyl Chloride → HCID 20275450, compound

HRID 647365Notes

Reaction equation

HRID 647365 reaction equation
[CH3:1][N:2]([CH3:13])[CH2:3][C:4]([CH3:12])([CH3:11])[CH2:5][NH:6][C:7](=[O:10])[CH:8]=[CH2:9].[CH3:14][Cl:15]>O>[Cl-:15].[C:7]([NH:6][CH2:5][C:4]([CH3:12])([CH3:11])[CH2:3][N+:2]([CH3:14])([CH3:1])[CH3:13])(=[O:10])[CH:8]=[CH2:9]

Participants

4

Reactant 2

HCID 6327Methyl ChlorideHCID 88388N-(3-(Dimethylamino)-2,2-dimethylpropyl)acrylamide

Product 1

HCID 20275450HCID 20275450, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Into a vigorously stirred 80° C. solution of 376 g N-(3-dimethylamino-2,2-dimethylpropyl)-acrylamide (TEMAPA of Example 1) in 320 g water, there was introduced over a period of 3.5 hours under a working pressure of 0.4 bar 103 g methyl chloride. An aqueous solution of the quaternary product was obtained.

Workup

  1. customAn aqueous solution of the quaternary product was obtained

Sources & evidence

ORD record
ord-874a02c681484ac38e61e9ec62217c94
Source dataset
uspto-grants-1983_10
Patent number
US04408073

Reaction notes

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