Sulfuric Acid → Sulfuric acid--prop-2-enamide (1/1)

Participants

Reaction Conditions

Reaction Steps

80 g N-(N',N',2',2'-tetramethylaminopropyl)-acrylamide was dissolved in 386 g water and acidified with 100 g 20% sulfuric acid. After addition of 100 g acrylamide, the solution was heated to 55° C. and polymerization was initiated with 80 mg azobisisobutyronitrile. After being allowed to stand for 3 hours, the gel-like copolymerization product was comminuted, dried and ground to give a white powder.

Provenance & Evidence