HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus pentachloride → HCID 20484914, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | HCID 13386238 | HCID 13386238 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20484914 | HCID 20484914 | — |
Reaction Steps
2-{4-[N-(1,7-Dichloroisoquinolin-3-yl)-N-methylamino]phenoxy}propionyl chloride was prepared by adding phosphorus pentachloride (1.07 g) portionwise to a solution of 2-{4-[N-(1,7-dichloroisoquinolin-3-yl)-N-methylamino]phenoxy}propionic acid (2.0 g) in dichloromethane at room temperature and stirring the reaction mixture for a period of 12 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04409017 |
| Source dataset | uspto-grants-1983_10 |
| ORD ID | ord-e8148651101645548af9ca87588e0b56 |
| Source note | uspto-grants-1983_10 |