HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 86739058, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 13386242 | HCID 13386242 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86739058 | HCID 86739058 | — |
Reaction Steps
A solution of 2-(dimethylamino)ethyl 2-{4-[N-(1,7-dichloroisoquinolin-3-yl)-N-methylamino]phenoxy}propionate in dichloromethane was added to a large excess of methyl iodide in dichloromethane. The mixture was stirred for 2 hrs at room temperature, then evaporated to give 2-dimethyl amino)ethyl 2-{4-[N-(1,7-dichloroisoquinolin-3-yl)-N-methylamino]phenoxy}propionate methyl iodide salt as yellow crystals mp 76° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04409017 |
| Source dataset | uspto-grants-1983_10 |
| ORD ID | ord-991afc3a61e0481d9411f0acf556fe4b |
| Source note | uspto-grants-1983_10 |