HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aminoacetamidine Dihydrobromide → 2-Amino-7-acetyl-6,7,8,9-tetrahydro-5H-pyrazino[2,3-d]azepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aminoacetamidine Dihydrobromide | HCID 16211382 | — |
| Reactant | 1-Acetyl-hexahydroazepine-3,4-dione | HCID 20436442 | — |
| Reactant | 1-Acetyl-hexahydroazepine-4,5-dione | HCID 20485032 | — |
| Product | 2-Amino-7-acetyl-6,7,8,9-tetrahydro-5H-pyrazino[2,3-d]azepine | HCID 13037043 | — |
Reaction Steps
This compound was prepared analogous to Example 13 by reacting a mixture of 1-acetyl-hexahydroazepine-4,5-dione and 1-acetyl-hexahydroazepine-3,4-dione (prepared from 1-acetylhexhydroazepine-4-ones by selenium dioxide oxidation in dioxane/water) with 2-amino-acetamidine dihydrobromide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04409220 |
| Source dataset | uspto-grants-1983_10 |
| ORD ID | ord-06b9fec509c543c0b17bd18ab19b07e5 |
| Source note | uspto-grants-1983_10 |