HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 20278223, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 12694098 | HCID 12694098 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 20278223 | HCID 20278223 | — |
Reaction Steps
A cold stirred solution of 1,3-dihydro-3-phenylspiro[benzo(c)thiophene-1,4'-piperidine], Example 4, and triethylamine in 50 ml of chloroform is treated dropwise with a solution of acetyl chloride in chloroform to provide 1'-acetyl-1,3-dihydro-3-phenylspiro[benzo(c)thiophene-1,4'-piperidine].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04409229 |
| Source dataset | uspto-grants-1983_10 |
| ORD ID | ord-3a5bc2a2949a494d9f0691b93c3105a1 |
| Source note | uspto-grants-1983_10 |