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HRID64759

反应详情

EQUATION

反应方程式

HRID 64759 的结构方程式

REACTANTS

反应物

2
结构：CC(N)CC#N
HCID123366

未命名化合物

结构：CC(C)S(=O)(=O)c1ccc(Oc2ccc([N+](=O)[O-])c([N+](=O)[O-])c2)c(Cl)c1
HCID20237345

未命名化合物

PRODUCTS

生成物

1
结构：CC(CC#N)Nc1cc(Oc2ccc(S(=O)(=O)C(C)C)cc2Cl)ccc1[N+](=O)[O-]
HCID20237378

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

A solution of 4.0 g of 2-chloro-4-isopropylsulphonyl-(3,4-dinitrophenoxy)benzene and 2,5 g of 3-aminobutyronitrile in 30 ml of acetonitrile was refluxed for 13 hours. After evaporation the residue was recrystallized from methanol. The desired product was obtained in a yield of 3.3 g; m.p. 132° C.

WORKUP

后处理

  1. customAfter evaporation the residue
  2. customwas recrystallized from methanol