HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-AMino-butyronitrile → HCID 20237378, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-AMino-butyronitrile | HCID 123366 | — |
| Reactant | 2-Chloro-4-isopropylsulphonyl-(3,4-dinitrophenoxy)benzene | HCID 20237345 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 20237378 | HCID 20237378 | — |
Reaction Steps
A solution of 4.0 g of 2-chloro-4-isopropylsulphonyl-(3,4-dinitrophenoxy)benzene and 2,5 g of 3-aminobutyronitrile in 30 ml of acetonitrile was refluxed for 13 hours. After evaporation the residue was recrystallized from methanol. The desired product was obtained in a yield of 3.3 g; m.p. 132° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04609753 |
| Source dataset | uspto-grants-1986_09 |
| ORD ID | ord-f14fe54d8cae4be49a411ae0a37b6218 |
| Source note | uspto-grants-1986_09 |