Tetrahydrofuran → HCID 20479397, compound

HRID 647605Notes

Reaction equation

HRID 647605 reaction equation
[C:1]([O:5][CH2:6][CH:7]=[CH:8][CH2:9][O:10][C:11]([CH3:14])([CH3:13])[CH3:12])([CH3:4])([CH3:3])[CH3:2].[O:15]1CCC[CH2:16]1>>[CH:16]([CH:8]([CH2:7][CH2:6][O:5][C:1]([CH3:3])([CH3:4])[CH3:2])[CH2:9][O:10][C:11]([CH3:14])([CH3:13])[CH3:12])=[O:15]

Participants

3

Reactant 2

HCID 8028TetrahydrofuranHCID 54076684HCID 54076684, compound

Product 1

HCID 20479397HCID 20479397, compound

Procedure

2,500 g of 1,4-bis-tert.-butoxybut-2-ene were hydroformylated in a conventional manner by means of an equimolar mixture of CO and H2 and 50 mg of the Rh catalyst mentioned in Example 1, in the presence of 2,000 g of tetrahydrofuran, at 100° C. and 650 bar for 24 hours.

Sources & evidence

ORD record
ord-cacdf7140eaa4d88bfbb3960f65f5e00
Source dataset
uspto-grants-1983_10
Patent number
US04409402

Reaction notes

Loading…