HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → 2-[(Benzyloxy)methyl]-2-ethyl-1,8-dioxaspiro[4.5]decane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | (2-Ethyl-1,8-dioxaspiro[4.5]decan-2-yl)methanol | HCID 13237164 | — |
| Product | 2-[(Benzyloxy)methyl]-2-ethyl-1,8-dioxaspiro[4.5]decane | HCID 13237165 | 24.8% |
Reaction Steps
Following procedures similar to those of Embodiments XVII-XIX, 2.50 g of 2-ethyl-1,8-dioxaspiro[4.5]decane-2-methanol was treated with 2.35 g of benzyl bromide in the presence of sodium hydride to yield 0.90 g of the desired product as a clear liquid, b.p. 130° C. (0.15 mm).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04410354 |
| Source dataset | uspto-grants-1983_10 |
| ORD ID | ord-98dc6749c37945448ccbc7605a17dfe2 |
| Source note | uspto-grants-1983_10 |