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HRID647748

反应详情

EQUATION

反应方程式

HRID 647748 的结构方程式

REACTANTS

反应物

3
结构：BrCc1ccccc1
HCID7498

alpha-Bromotoluene

C7H7Br

结构：[H-].[Na+]
HCID24758

Sodium hydride

HNa

结构：CCC1(CO)CCC2(CCOCC2)O1
HCID13237164

(2-Ethyl-1,8-dioxaspiro[4.5]decan-2-yl)methanol

C11H20O3

PRODUCTS

生成物

1
结构：CCC1(COCc2ccccc2)CCC2(CCOCC2)O1
HCID13237165

2-[(Benzyloxy)methyl]-2-ethyl-1,8-dioxaspiro[4.5]decane

C18H26O3

收率 24.8%

PROCEDURE

实验过程

Following procedures similar to those of Embodiments XVII-XIX, 2.50 g of 2-ethyl-1,8-dioxaspiro[4.5]decane-2-methanol was treated with 2.35 g of benzyl bromide in the presence of sodium hydride to yield 0.90 g of the desired product as a clear liquid, b.p. 130° C. (0.15 mm).