HRID647785

反应详情

EQUATION

反应方程式

HRID 647785 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A suspension of 3.11 g. of 1,4-dihydroxy-5,8-bis[[2-(2-hydroxyethylamino)ethyl]amino]anthraquinone [prepared as described in Example 1(A)] in 55 ml. of toluene containing 2.0 g. of pyrrole-2-carboxaldehyde is stirred and refluxed as for Example 1(B). The hot solution is filtered. The filtrate is concentrated and allowed to stand at room temperature. The title compound separates as blue-black crystals.

WORKUP

后处理

  1. additionA suspension of 3.11 g
  2. temperaturerefluxed as for Example 1(B)
  3. filtrationThe hot solution is filtered
  4. concentrationThe filtrate is concentrated
  5. customto stand at room temperature