HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → HCID 14209981, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | HCID 12658724 | HCID 12658724 | — |
| Solvent | Toluene | HCID 1140 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 14209981 | HCID 14209981 | — |
Reaction Steps
From 4,9-dihydro-1-methyl-10H-thieno[3,4-b][1,5]benzodiazepin-10-one and phosgene in a mixture of dioxane and toluene, 4-chlorocarbonyl-4,9-dihydro-1-methyl-10H-thieno[3,4-b][1,5]benzodiazepin-10-one was obtained, m.p. 235°-236° C. (chloroform);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04410527 |
| Source dataset | uspto-grants-1983_10 |
| ORD ID | ord-6b5e22710614478d84cc944b3b95b3b8 |
| Source note | uspto-grants-1983_10 |