Sodium borohydride → HCID 178512085, compound

Participants

Reaction Steps

In this example, 600 mg of sodium borohydride is added to a suspension of 715 mg of the product obtained in Example 9 in 30 ml of ethanol at room temperature. After completion of the addition, the reaction mixture is concentrated. The residue is mixed with water, and the crystals deposited are separated by filtration and dried. The crude crystals are recrystallized from methanol to obtain 632 mg of the desired product.

Provenance & Evidence