Triethanolamine → HCID 86738296, compound

HRID 647828Notes

Reaction equation

HRID 647828 reaction equation
Cl.Br[CH:3]([CH2:6][NH:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])C#N.[N:13](CCO)(CCO)[CH2:14]CO>>[C:14]([CH:9]([CH2:10][CH2:11][CH3:12])[CH2:8][N:7]1[CH2:6][CH2:3]1)#[N:13]

Participants

3

Reactant 2

HCID 7618TriethanolamineHCID 86738297HCID 86738297, compound

Product 1

HCID 86738296HCID 86738296, compoundYield 43%

Procedure

reaction of 2-bromo-3-n-pentylaminopropionitrile hydrochloride (prepared by reacting 2,3-dibromopropionitrile with n-pentylamine; m.p. 133°-135° C.) with triethanolamine gives 2-cyano-n-pentylaziridine; b.p.0.3 : 50°-52° C.; yield 43% of theory;

Sources & evidence

ORD record
ord-c450ee45d332410a8a66d36e98ccb9fa
Source dataset
uspto-grants-1983_10
Patent number
US04410532

Reaction notes

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