HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → 4-Ethyl-5-[4-(1-piperidinyl)benzoyl]-2-imidazolidinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 5-Ethyl-4-(4-fluorobenzoyl)-2-imidazolidinone | HCID 20484362 | — |
| Product | 4-Ethyl-5-[4-(1-piperidinyl)benzoyl]-2-imidazolidinone | HCID 20484363 | — |
Reaction Steps
A suspension of 10 g of 5-ethyl-4-(4-fluorobenzoyl)-2-imidazolidinone in 30 ml piperidine is stirred at reflux for 24 hours. Excess piperidine is evaporated under reduced pressure and the residue is purified by crystallization from alcohol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04410540 |
| Source dataset | uspto-grants-1983_10 |
| ORD ID | ord-4ddbf90ac6ac4b019dcfaf4b60cee3f7 |
| Source note | uspto-grants-1983_10 |