HRID647834

反应详情

EQUATION

反应方程式

HRID 647834 的结构方程式

PROCEDURE

实验过程

A suspension of 10 g of 5-ethyl-4-(4-fluorobenzoyl)-2-imidazolidinone in 30 ml piperidine is stirred at reflux for 24 hours. Excess piperidine is evaporated under reduced pressure and the residue is purified by crystallization from alcohol.

WORKUP

后处理

  1. temperatureat reflux for 24 hours
  2. customExcess piperidine is evaporated under reduced pressure
  3. customthe residue is purified by crystallization from alcohol